Document ppGY815wO5knzMydJX4XZj9Rk

uate CertainTeecO March 30, 1977 Subject FIBER RELATIVE STRENGTHS 10 See Below i A Mr. F. E. Hawkins location and mail code See Below Location and mail code VF P&PG #8 Mr. R. Wingartner Mr. J. L. Anderson Mr. H. G. Benhardt Mr. S. G. Leyshock Mr. N. Rhoades Mr. L. C. Kurfuerst Mr. M. R. Streepy Mr. T. A. Dougherty Mr. J. P. McGinley Mr. J. W. Walker Santa Clara #256 Hillsboro #257 Ambler #258 St. Louis #259 Riverside #260 VF P&PG #8 VF P&PG #8 VF P&PG #2B VF P&PG #2B VF P&PG #8 PLAINTIFF'S EXHIBIT He have reviewed all of our relative strength determinations made since August 1974 and have collected the results and test data in one report 1976 Relative Strengths for Asbestos Fiber which is attached. Reading of the first thirteen pages of the report should yield an understanding of the fiber test and of the precision of the results. The remaining pages cover the raw data from the laboratory and can be examined if you wish further information on the tests. FEH/kem Enclosure - 1976 Relative Strengths for ABbestos Fiber RECEIVED t 1377 i-as-ooos i* CTD000861 rn 1976 Relative Strengths for Asbestos Fiber LJ \/. $. /^i aj2o -r>uis John A. Malone March 21, 1977 prprrjycQ " 1 1777 CTD000862 1976 Relative Strength Values for Asbestos Fibers Objective of Report In 1976 the relative strengths of asbestos fibers were re-evaluated and the values were Increased by an average of about 13 per cent. There has been some reluctance to fully accept these new values. The objective of this report is to 6how how the new values were determined, to show the reproducibility of the data, and to show how the new values can predict the relative strength of fiber blends processed in the pipe plants. It is hoped that readers of the report will become convinced that the 1976 relative strengths are reasonable values and can be used with confidence. Description of Procedure Historically the term "Relative Strength" was first used in 1953 to define the asbestos-cement reinforcing characteristics of an asbestos fiber as a percentage of strength supplied by a specially prepared C&G/3 sample which was chosen as standard. The laboratory test procedure used to determine this relative strength is detailed in CertainTeed Technical Specification TM-7, and is included in the Chrysotile Asbestos Test Manual published jointly by the Asbestos Textile Institute and the Quebec Asbestos Mining Association. In the evaluation of a fiber for relative strength, test cakes containing a specified amount of asbestos, cement, and pulverized silica are prepared under controlled conditions by mixing the dry materials with water, filtering the resulting slurry under vacuum in a Buchner funnel, and pressing the filtered cakes in a confined mold. The pressed samples are then cured under controlled humidity conditions, and are finally autoclaved using saturated steam. After curing, the cakes are dried and CTD000863 2 then tested in flexure in two directions. From the average breaking load, the reinforcing characteristics of the fiber being evaluated relative to the standard are determined and expressed as relative strength. Aside from following the specified procedure in detail, it is essential for reliable results that a uniform slurry distribution be obtained in the Buchner funnel during cake formation, and that damage to the wet samples due to improper handling be carefully avoided. Standard Fiber Since the original supply of standard C&G/3 is almost gone, a new fiber (Cassiar AX) was standardized against the C&G/3. The results obtained are lis-ted in the appendix on page 15. Three tests were run, each consisting of nine standard C&G/3 cakes and six Cassiar AX cakes. The relative strengths obtained were as follows: Test 1 Test 2 Test 3 Average 93 93 96 94 This average of 94 was used for the standard Cassiar AX in determining the 1976 relative strength values. Example of Relative Strength Determination (Relative Strength of Cassiar AK) In practice, three standard cakes are prepared at three different fiber contents for a total of nine cakes to establish an average flexural breaking load versus fiber percentage curve for the standard. Using the current standard Cassiar AX with a relative strength of 94, the following is an example determination of the relative strength for Cassiar AK. CTD000864 TABLE 1 Standard Cassiar AX - Flexural Strength Sample 3% Fiber pounds average 1 82 83.0 84 2 106 104.0 102 3 107 103.5 100 Median Average 101 97 9% Fiber pounds average 152 156.5 161 157 150.0 143 152 165.5 179 155 157 15% Fiber pounds average 226 219.0 212 216 221.0 226 232 233.5 235 226 225 Cassiar AK - Flexural Strength Sample 1 2 3 Median Average 15% Fiber pounds 249 281 259 275 257 292 267 269 average 265.0 267.0 274.5 CTD000865 4 A set of standard cakes was run to determine the strength contribution of the cement and silica and the breaking load for the 15 per cent standard fiber cakes. At the same time, three cakes were made containing 15 per cent of the Cassiar AK. Each cake was broken twice. After the first break the two halves were placed to gether and the cakes were broken into quarters. The results obtained are tabulated in Table 1. The data for the standard were then plotted^Figure l^and the breaking loads for the 0 per cent and 15 per cent fiber points determined from the graph. (When the data is scattered from a straight line, the graph is constructed by the least squares method in order to get the best fit for the data. In the present case, this was not necessary). "Standard Cassiar AX" Breaking Load 157. Standard AX 225 pounds Breaking Load 0% Fiber 6A pounds Breaking Load 15% Cassiar AK 269 pounds Relative Strength Standard AX 94 Relative Strength Cassiar AK = (269 - 64) (94)/(225 - 64) = 120 Reproducibility of Relative Strength Tests Inherent in the test procedure are differences in strength caused by variations in curing conditions, variations in the cement, silica, and fiber used, variations in drying conditions, and the ever present unknown factors. It has been found, howeve that these effects tend to cancel out when a fiber is always evaluated against a standard, and although the absolute strengths might vary, the relative results hold fairly constant. As an example are the following results for Clinton CY which was tested three times using the same fiber sample. CTD000867 6 Breaking Load CY Breaking Load Standard (1) Breaking Load 0% Fiber (1) Relative Strength Raw Data Appendix Page Test 1 210 225 64 85 19 Test 2 208 226 60 84 20 Test 3 218 234 89 84 21 It should be noted in the foregoing that the breaking loads for the 0 per cent and 15 per cent fiber points in the case of the standard were taken from the average flexural breaking load versus fiber percentage curve. The breaking load for the 15 per cent fiber point used in the Test 3 relative strength calculation is 4 pounds lower than the average experimental value for 15 per cent standard Cassiar AX. This results from the influence of the 3 per cent and 9 per cent standard fiber cakes on the average curve. Statistical Evaluation of Relative Strength Values Another way of looking at the accuracy of the test is to compute the probability of being off by 5 relative strength units. This can be done roughly by using all the data we have on test fibers and the standard fiber and calculating an estimate of the variance of the average breaking loads. In making a fiber strength evaluation, the following cases can occur; Case Average Breaking Load of Test Cakes Standard Test Fiber Effect on Relative Strength Value 1 high high 2 low low 3 high low 4 low high minimal minimal gives low values gives high valuea Cases 1 and 2 give relative strengths closer to the true values than Cases 3 and 4. If Case 3 occurs, we will rate the fiber on the low side and therefore will CTD000868 7 overformulate. Case 4 would result in underformulating since the relative strength of the fiber blend would actually be lower than calculated. This worse case will be looked at in the following. We will calculate an estimate of how often a relative strength value can be expected to be 5 units higher than its true value. After the estimate is completed, we will calculate the effect of a 5 unit high fiber rating on the effectiveness of furnish. Using the data for the standard AX and the test fibers given in the Appendix, the variance of each cake average test break from the average breaking load for all the cakes in that test was calculated. 2 S= -2 (X - X) N-1 X = Average of the 2 breaking loads for a cake X = Average breaking loads for all cakes of the test N = Total number of cakes - degrees of freedom used in calculating averages = 261 - 75 = 186 S2 = 14,068.86 "*155-- = 76,047 S = >/76.047 =* 8.72 Then since we use 3 cakes in a test, the standard deviation of the average is: S = 8.72 = 5.03 lbs. X TT = Now we will calculate what changes in breaking load of the test and standard fibers would result in a 5 unit change in relative strength. To do this, we will take a test case which is similar to many of our fibers. CTD000869 8 Assume: 1) Test fiber has a true relative strength of 105 2) Standard fiber cake break at an average of 225 3) 0% fiber cake break correction of 64 pounds Then: X - 64 225 - 64 X 94 = 105 X = 244 breaking load of test fiber The next calculation is what the breaking load of the test fiber and of the standard fiber must change to give a 5 unit increase in the test fiber relative strength. It is assumed both fibers vary by the same amount, the test fiber high the standard fiber low. 244 + Y - 64 x 94 - 110 225 - Y - 64 Y = 3.87 lbs Therefore, if the average breaking load is 3.87 lbs high for the test fiber and 3.87 lbs low for the standard fiber, the relative strength will be 5 units high. Now to calculate the probability of this difference to occur. Using Sx as representative of Z = 3.87 = 3.87 = .7694 5.03 The area under the normal distribution curve from Z-> Goto Z = 0.769 is .2212. Thus there are 22.12 chances out of 100 that an average of the breaking load of 3 cakes will be more than 3.87 lbs high or low. The possibility that the test fiber would be high by this amount at the same time the standard fiber would be low by that amount is then calculated by: CTD000870 9 22.12 X 22.12 = .0489 100 100 or 1 chance out of 20.4 Thus there is about 1 chance out of 20 that we would rate a fiber 5 units more than its actual value. Then to calculate how much a change of 5 units would make in the effectiveness of furnish - Assume - 1) Relative Strength of Fiber Blend = 100 2) Amount of over-rated fiber 25% 3) Effectiveness of Furnish 1550 4) All other fibers rated correctly so there are no compensating errors. Relative Strength of Fiber Blend would be reduced by: (.25 x 110 - .25 x 105) = 1.25 units The fiber blend would then have a relative strength of 98.75 units and the Effectiveness of Furnish would be 1531 instaed of 1550. This is a small variable in making pipe. Old and 1976 Relative Strengths Table II is a tabulation of the relative strength figures now in use compared with the old values. Note that the 1976 relative strengths are higher than the old values. The reason for this increase is mainly due to greater opening, although it may also result CTD000871 Fiber Clinton Clinton Cassiar Russian Cassiar Asb. Corp. Blue BT/AD Havelock JM JM Russian Russian Bell Blue ML6 Cassiar Asb. Corp. Asb. Corp. C&G C&G C&G Clinton CT CY AK P-5 AX 40 4 5 *2 - ZS P-4 P-3 4/'-Set' AS 44TJ J&C ir) 4r) 5 4 3 CP Relative Strength 92 65 110 70 90 94 85 95 70 90 90 97 90 96 97 102 90 90 104 120+ 100 CTD000872 Clinton CT Clinton CY Cassiar AK Cassiar AS Cassiar AX Cassiar AZ JM 4T-30 JM 5R-28 Corp. 4D Corp. 4j Corp. 4T Russian P-5 Pacific 4T Pacific 5R ML-6 Blue BT/AD Blue Old Values 92 65 110 97 90 73 90 70 94 102 90 70 90 70 96 85 TABLE II Relative Strengths 1976 Values 104 84 120 114 105 83 93 76 106 108 107 81 105 75 106 94 1976 T&N Surface Area sq.cm./g. 8,300 9,900 9,000 9,000 9,000 11,200 16,200 13,300 11,900 9,500 12,200 12,700 12,400 12,300 13,300 ___ Raw Data for 1976 Value Appendix Page 18 19-21 22 23 24 25 26 27 28 . 29 30 31-33 34 35 36 ---- CTD000873 11 in the case of some fibers from improvements at the mine. Relative Strength of Plant Prepared Fiber Blends (Calculated versus Experimental Values) Over the years, many tests have been run on plant processed fiber blends. In these evaluations, test cakes containing 15 per cent of the blend were prepared and the relative strengths determined in the same manner as for individual fibers. The results of these tests are given in Table III, where they are compared with the strengths predicted by using the old and the 1976 relative strength values. Following is an example calculation of these predicted strengths for Blend 17 received from Plant 256 during October 1974. Per Old Cent Values Per Cent 1976 Values Cassiar AS Clinton CT Cassiar AX Clinton CY Total 20 X 30 X 15 X 35 X 100 97 - 1940 92 = 2760 90 = 1350 65 - 2275 8325 20 X 30 X 15 X 35 X 100 114 = 2280 104 = 3120 105 = 1575 84 = 2940 9915 Predicted Strength (using old values) 8325/100 = 83 Predicted Strength (using 1976 values) 9915/100 = 99 Experimental Relative Strength 97 The data in Table III are arranged in chronological order. Note that the relative strengths calculated with the old values were always lower than the relative strengths determined experimentally in the laboratory. The figures in parentheses indicate those cases where the relative strengths determined experimentally in the laboratory were lower than the relative strengths calculated with the 1976 values. Note that all but two of these cases occurred in 1974 when the plants were running with low surface areas. After 1974 the plants were opening the fibers to a CTD000874 TABLE III 12 Blench Plant 256 17 257 86 258 85 259 76 260 86 257 115 256 71 257 187 258 170 259 62 260 84 257 Std. 258 stdn 259 std-S 260 Std. 256 20X 256 20 258 64 258 64 258 94 257 61 258 144 260 49 257 105 257 125 Laboratory Calcalated Strength Date 10/74 10/74 10/74 10/74 10/74 8/75 12/75 12/75 12/75 12/75 12/75 2/76 3/76 3/76 2/76 3/76 3/76 5/76 5/76 6/76 7/76 8/76 9/76 9/76 11/76 Laboratory Relative Strength (97) (100) (94) (94) (95) 101 100 113 (102) 105 106 118 108 110 110 106 110 99 109 (98) 120 104 120 114 111 Calculated. Strength Old 1976 Values Values 83 99 90 102 87 95 91 101 88 101 89 101 85 99 90 103 95 109 92 104 87 100 89 102 89 102 89 102 89 102 89 100 86 101 88 99 88 99 88 100 88 101 87 97 88 101 86 97 93 105 TOT Surface Area sc], cmffg. 8,000 8,400 10,300 8,000 9,100 11,400 9,900^ 11,400 9,700 9,300 9,300 11,800 8,800 9,900 10,400 9,100 9,100 9,300 11,000 12,000 10,900 10,300 10,600 11,400 12,700 Raw Data Appendix Page 41 42 42 45 44-46 47 47 47 49 49 49 51 51 52 52 53 53 54 54 55 56 57 58 58 60 < Blends are given in the Appendix starting on page 37. Passed through two willow mills in series. Same fiber blend used in all plants. Appendix IV page 39. CTD000875 13 greater degree and in only two cases out of twenty were the relative strengths determined experimentally in the laboratory lower than expected by calculations based on the 1976 figures. On the average after 1974 the relative strengths of the plant blends were about 7 per cent higher than the strengths calculated with these 1976 figures. Considering the things that can happen between dumping bags of fiber into a mixer and getting a sample from the willow, these data indicate that the plants are doihg a good job and that the relative strength values are a reasonably accurate tool for use in formulating fiber blends. CTD000876 APPENDIX I Initially 3, 9, and 15 per cent Standard Cassiar AX samples were prepared to establish the standard curve for relative strength evaluations. Because of difficulty in handling the wet test cakes .containing 3 per cent fiber, however, the percentages were later changed to 5, 10 and 15 per cent. Further, average flexural breaking loads were used initially in relative strength calculations, but median values were used in later work as being statistically more reliable with the relatively small number of samples involved. CTD000877 APPENDIX II Sample 1 2 3 Median Average Standardization of Cassiar AX vs C&G/3 Standard Standard Cassiar AX - Test #1 Standard C&G/3 (1953 Sample) - Flexural Strength 3% Fiber pounds average 9% Fiber pounds average 157. Fiber pounds average 93 91.0 89 80 85.5 91 84 77.0 70 165 156.0 147 176 174.5 173 170 167.5 165 233 239.0 245 253 238.5 224 238 251.0 264 87 168 242 85 166 243 Standard Cassiar AX - Flexural Strength Sample 157 Fiber pounds average 1 210 222.5 235 2 229 230.5 232 3 210 233.0 256 4 222 232.5 243 5 221 232.0 243 6 247 233.0 219 Median Average 231 231 From Average Standard C&G/3 Curve (using average values) Breaking Load 157. C&G/3 Breaking Load 07. Fiber Relative Strength Std. AX 244 pounds 46 93 CTD000878 Sample 1 2 3 Median Average Standard Cassiar AX - Test #2 Standard C&G/3 (1953 Sample) - Flexural Strength 37. Fiber pound:s average 97. Fiber pounds average 157. :Fiber pounds average 90 92.5 95 94 91.5 89 69 77.0 85 166 156.5 147 170 169.5 169 140 143.0 146 269 235.5 202 262 254.0 246 237 238.5 240 90 157 243 87 156 243 Standard Cassiar AX - Flexural Strength Sample 157. Fiber pounds average 1 233 237.5 242 2 236 225.0 214 3 229 236.5 244 4 240 224.0 208 5 216 223.0 230 6 208 214.0 220 Median Average 230 227 From Average Standard C&G/3 Curve (Using average values) Breaking Load 157. C&G/3 Breaking Load 07. Relative Strength Std. AX 240 pounds 45 93 CTD000879 Sample 1 2 3 Median Average Standard Cassiar AX - Test #3 Standard C&G/3 (1953 Sample) - Flexural Strength 37. Fiber pounds average 89 82.0 75 65 68.5 72 68 69.5 71 72 73 97. Fiber pounds average 150 147.5 145 158 159.0 160 162 137.5 113 154 148 157. Fiber pounds average 237 227.5 218 217 229.5 242 210 227.5 245 228 228 Standard Cassiar AX- Flexural Strength Sample 1 2 3 4 5 6 pounds 224 211 243 224 234 212 225 210 220 206 217 215 157. Fiber average 217.5 233.5 223.0 217.5 213.0 216.0 Median Average 219 220 From Average Standard C&G/3 Curve (Using average values) Breaking Load 157. C&G/3 Breaking Load 0% Fiber Relative Strength Std. AX 228 pounds 34 96 CTD000880 APPENDIX III Relative Strength Tests for Fibers Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 37. Fiber pounds average 97. Fiber pounds average 157. Fiber pounds average 82 83.0 84 106 104.0 102 107 103.5 100 152 156.5 161 157 150.0 143 152 165.5 179 226 219.0 212 216 221.0 226 232 233.5 235 101 155 226 97 157 225 Clinton CT - Flexural Strength Sample 157. Fiber pounds average 1 238 235.0 232 2 249 249.0 249 3 246 241.5 237 Median Average 242 242 From Average Standard AX Curve (Using average values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength CT 225 pounds 64 104 CTD000881 Clinton CY Fiber - Test #1 Standard Cassiar AX - Flexural Strength Same standard as for Clinton CT Fiber Appendix III Page 18. Clinton CY - Flexural Strength Sample 157. Fiber pounds average 1 205 206.5 208 2 207 213.5 220 3 197 211.0 225 Median Average 208 210 From Average Standard AX Curve (Using average values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength CY 225 pounds 64 85 CTD000882 Clinton CY Fiber - Test #2 Standard Cassiar AX - Flexural Strength Same as standard for JMR-28 Fiber Appendix III Page 27. Clinton CY - Flexural Strength Sample 157. Fiber pounds average 1 2 3 Median Average 206 196 232 198 216 199 203 208 201.1 215.0 207.5 From Average Standard AX Cruve (Using average values) Breaking Load 15% Std. AX Breaking Load 0% Fiber Relative Strength CY 226 pounds 60 84 20 CTD000883 Clinton CY Fiber - Test #3 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 3% Fiber pounds average 97. Fiber pounds average 157. Fiber pounds average 111 125.0 139 133 128.5 124 128 114.5 101 143 156.0 169 174 164.5 155 179 176.5 174 225 238.5 252 259 248.0 237 220 228.5 237 126 172 237 123 166 238 Clinton CY - Flexural Strength Sample 157. Fiber pounds average 1 212 218.5 225 2 204 216.5 229 3 243 219.0 195 Median Average 219 218 From Average Standard AX Curve (Using average values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength CY 234 pounds 88 84 CTD000884 Cassiar AK Fiber Standard Cassiar AX - Flexural Strength Same Standard as Clinton CT Fiber Appendix III Page 18. Cassiar AK - Flexural Strength Sample 15% Fiber pounds average 1 249 265.0 281 2 259 267.0 275 3 257 274.5 292 Median Average 267 269 From Average Standard AX Curve (Using average values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength AK 225 pounds 64 120 CTD000885 Cassiar AS Fiber Sample 1 2 3 Median . Standard Cassiar AX - Flexural Strength 37. Fiber pounds average 9% Fiber pounds average 157. Fiber pounds average 73 74.5 76 76 72.0 68 90 83.5 77 143 139.5 136 157 140.0 123 141 141.5 142 212 213.5 215 193 205.5 218 202 198.0 194 76 142 77 140 207 206 Cassiar AS - Flexural Strength Sample 15% Fiber pounds average 1 229 233.0 237 2 234 242.5 251 3 250 .249.5 249 Median 243 242 From Average Standard AX Curve (Using Median Values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength AS 208 pounds 44 114 CTD000886 Cassiar AX Fiber Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 37. Fiber pounds average 97. Fiber pound s average 157. Fiber pounds average 92 80.0 68 71 82.5 94 96 88.5 81 157 152.5 148 143 142.5 142 152 146.0 140 209 207.0 205 225 211.0 197 214 218.0 222 87 146 212 84 147 212 Cassiar AX - Flexural Strength Sample 157. Fiber pounds average 1 226 226.0 226 2 259 250.0 241 3 212 212.5 213 Median Average 226 230 From Average Standard AX Curve (Using average values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength AX 211 pounds 51 105 CTD000887 Cassiar AZ Fiber Sample 1 2 3 Median Standard Cassiar AX - Flexural Strength 3% Fiber pounds average 9% Fiber pounds average 15% Fiber pounds average 64 69.0 74 79 79.0 79 71 66.5 62 143 144.0 145 148 141.0 134 140 144.5 149 197 204.5 212 205 206.0 207 219 230.0 241 73 144 210 72 143 214 Cassiar AZ - Flexural Strength Sample pounds 15% Fiber average 1 187 181.0 175 2 173 184.0 195 3 205 201.5 198 Median Average 191 189 From Average Standard AX Curve (Using median values) Breaking Load 15% Std. AX Breaking Load 0% Fiber Relative Stemgth AZ 212 pounds 40 83 CTD000888 Sample 1 2 3 Median JM 4T-30 Fiber Standard Cassiar AX - Flexural Strength 3% Fiber pounds average 9% Fiber pounds average 15% Fiber pounds average 93 88.5 84 82 80.0 78 80 79.5 79 155 175 170 146 147 *140 165.0 158.0 143.5 245 234.0 223 235 228.0 221 222 217.5 213 81 151 223 83 156 227 Sample 1 2 3 4 5 6 Median Average JM 4T-30 - Flexural Strength pounds 15% Fiber average 203 221.0 239 219 216.0 213 240 237.5 235 203 213.5 224 223 229.0 235 240 234.0 228 226 225 From Average Standard AX Curve (Using average values) Breaking Load 15% Std. AX Breaking Load 0% Fiber Relative Strength JM 4T-30 227 pounds 47 93 CTD000889 JM 5R-28 Fiber Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 37. Fiber pounds average 97. Fiber pounds average 157. Fiber pounds average 67 78.5 90 85 87.0 89 98 106.0 114 155 158.0 246 226.5 161 207 159 161.0 243 218.0 163 193 168 167.5 212 223.5 167 235 90 162 224 91 162 223 JM 5R-28 - Flexural Strength Sample pounds 157. Fiber average 1 208 202.5 197 2 203 193.5 184 3 171 187.0 203 Median Average 200 194 From Average Standard AX Curve (Using Average Values) Breaking Load 157. Std. AX Breaking Load 0% Fiber Relative Strength JM 5R-28 226 pounds 60 76 CTD000890 Corp. 4D Fiber Sample 1 2 3 Median Average Standard C&G/3 (1953 Sample) - Flexural Strength 37. Fiber pounds average 97. Fiber pounds average 157. Fiber pounds average 95 76.5 58 61 70.5 80 85 84.0 83 154 150.5 147 181 166.5 152 137 148.5 160 219 212.0 205 231 226.5 222 215 220.0 225 82 153 221 77 155 220 Corp. 4D - Flexural Strength Sample pounds 157. Fiber average 1 246 245.5 245 2 233 243.5 254 3 233 222.5 212 4 239 220.0 201 5 233 231.5 230 6 249 237.5 226 Median Average 233 233 From Average Standard C&G/3 Curve (Using Average Values) Breaking Load 157. C&G/3 Breaking Load 0L Fiber Relative Strength Corp. 4D 223 pounds 44 106 CTD000891 Corp. 4j Fiber Standard C&G/3 (1953 Sample) - Flexural Strength Same Standard as Corp. 4D Fiber Appendix III Page 28. Corp. 4J - Flexural Strength Sample 1 2 3 4 5 6 Median Average 157. Fiber pounds 222 220 212 247 243 252 230 223 235 255 243 260 239 237 average 221.0 229.5 247.5 226.5 245.0 251.5 From Average Standard C&G/3 Curve (Using Average Values) . Breaking Load 157. C&G/3 Breaking Load 07. Fiber Relative Strength Corp. 4J 223 pounds 44 108 CTD000892 Corp. AT Fiber Standard Cassiar AX - Flexural Strength Same standard as Cassiar AX Fiber page 24. Sample 1 2 3 Median Average Corp. 4T - Flexural Strength 15% Fiber pounds average 252 235.5 219 233 234.0 235 229 228.5 228 231 233 From Average Standard AX Curve (Using Average Values) Breaking Load 15% Std. AX Breaking Load 0% Fiber Relative Strength Corp. 4T 211 pounds 51 107 CTD000893 Russian P-5 Fiber - Sample #1 Sample 1 2 3 Median Standard Cassiar AX - Flexural Strength 37. Fiber pounds average 97. Fiber pounds average 157. Fiber pound s average 75 86.5 98 84 87.0 90 87 91.0 95 157 149.0 141 161 153.0 145 160 158.5 157 214 229.5 245 260 236.0 212 202 212.5 223 89 157 219 88 154 226 Russian P-5 - Flexural Strength Sample pounds 157. Fiber average 1 211 199.0 187 2 238 214.5 191 3 224 213.5 203 Median Average 207 209 From Average Standard AX Curve (Using Average Values) - Breaking Load 15% Std. AX ' Breaking Load 0% Fiber Relative Strength Russian P-5 225 pounds 52 85 CTD000894 Russian P-5 Fiber - Sample #2 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 37. Fiber pounds average 80 80.0 80 74 78.5 83 73 82.0 91 80 80 97. Fiber pounds average 142 156.5 171 165 149.5 134 148 151.0 154 151 152 157. Fiber pounds average 237 235.0 233 235 215.5 196 221 218.0 215 227 223 Russian P-5 - Flexural Strength Sample 157. Fiber pounds average 1 178 179.0 180 2 181 179.5 178 3 193 183.0 173 Median Average 179 181 From Average Standard AX Curve (Using Average Values) - Breaking Load 157. Std. AX ' Breaking Load 0% Fiber Relative Strength Russian P-5 224 pounds 45 71 CTD000895 Russian P-5 - Sample #3 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 37. Fiber pounds average 97. Fiber pound s average 157. Fiber pounds average 65 68.5 72 78 73.5 69 82 75.0 68 146 142.5 139 145 138.5 132 135 139.0 143 243 219.5 196 214 208.0 202 225 216.5 208 71 141 211 72 140 215 Russian P-5 - Flexural Strength Sample pounds 157. Fiber average 1 210 207.0 204 2 208 199.5 191 3 221 201.0 181 Median Average 206 203 From Average Standard AX Curve (Using Average Values) Breaking Load 157 Std. AX Breaking Load 07. Fiber Relative Strength Russian P-5 214 pounds 35 88 CTD000896 Pacific 4T Fiber Standard Cassiar AX - Flexural Strength Same standard as Cassiar AS Fiber Appendix III Page 23. Pacific 4T - Flexural Strength Sample 15% Fiber pounds average 1 218 223.0 228 2 225 216.0 207 3 235 231.5 228 Median Average 227 224 From Average Standard AX Curve (Using Median Values) Breaking Load 15% Std. AX Breaking Load 0% Fiber Relative Strength Pacific 4T 208 pounds 44 105 CTD000897 Pacific 5R Fiber Standard Cassiar AX - Flexural Strength Same standard as Cassiar AS Fiber Appendix HI Page 23. Pacific 5R - Flexural Strength Sample 15% Fiber pounds average 1 175 179.5 184 2 165 157.5 150 3 174 174.0 174 Median Average 174 170 From Average Standard AX Curve (Using Median Values) Breaking Load 157. Std. AX Breaking Load 0% Fiber Relative Strength Pacific 5R 208 pounds 44 75 CTD000898 ML-6 Blue Fiber Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 37. Fiber pounds average 97. Fiber pounds average 157. Fiber pounds average 84 81.0 78 71 68.5 66 110 105.0 100 164 154.5 145 154 156.5 159 145 155.0 165 223 217.0 211 213 213.5 214 224 219.5 215 81 157 215 85 155 217 ML-6 Blue - Flexural Strength Sample 157. Fiber pounds average 1 238 239.0 240 2 277 262.0 247 3 235 229.0 223 Median Average 239 243 From Average Standard AX Curve (Using Median Values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength ML-6 217 pounds 49 106 CTD000899 APPENDIX IV Plant Blend Compositions Plant 256, Blend 17-10/74 Casslar AS 20.0% Clinton CT 30.0 Cassiar AX 15.0 Clinton CY 35.0 Plant 257, Blend 86-10/74 Clinton CT 37.5% Cassiar AK 8.3 Cassiar AX 8.3 Clinton CY 16.7 S Blue 25.0 ML-6 Blue 4.2 Plant 258, Blend 85-10/74 Cassiar AK 7.6% Cassiar AX 11.4 S Blue 4.2 Clinton CY 11.4 BT/AD Blue 12.4 JM 5R-28 7.6 JM 4T-30 45.4 Plant 259, Blend 76-10/74 Cassiar AK 16.6% Clinton CT 16.6 Bell 4T-500 16.7 JM 4T-500 16.7 Clinton CY 11.1 JM 5R-28 5.6 ML-6 Blue 16.7 Plant 260, Blend 86-10/74 Clinton CY 18.9% Clinton CT 34.0 BT/AD Blue 16.7 ML-6 Blue 3.8 Cassiar AK 11.4 Cassiar AX 15.2 CTD000900 Plant 257, Blend 115-8/75 HVL/3 5.27. HVL/4 41.6 Russian P-3 14.5 Russian P-5 14.2 Clinton CY 9.4 BT/AD Blue 10.4 TA/K Blue 4.7 Plant 256, Blend 71-12/75 Cassiar AS 14.97. Cassiar AK 5.0 HVL/4 5.5 Clinton CT 39.9 Clinton CY 19.9 Russian P-5 14.8 Plant 257, Blend 187-12/75 Cassiar AK 22.5 Clinton CT 27.1 Cassiar AX 18.0 Clinton CY 18.0 BT/AD Blue 9.9 ML-6 Blue 4.5 Plant 258, Blend 170-12/75 Cassiar AK 14.77. Cassiar AX 14.7 Clinton CY 18.3 Clinton CT 14.7 JM 5R-28 7.3 ML-6 Blue 7.3 C&G/3 23.0 Plant 259, Blend 62-12/75 Cassiar AK 22.% Clinton CT 50.0 Clinton CY 16.7 ML-6 Blue 11.1 CTD000901 Plant 260, Blend 84-12/75 Clinton CY 30.57. Clinton CT 42.0 Cassiar AK 19.1 BT/AD Blue 8.4 Plants 257, 258, 259, 260 St Cassiar AK 17.97. Clinton CT 49.4 Clinton CY 17.9 BT/AD Blue 14.8 Plant 256, Blend 20X-3/76 Cassiar AS 10.07. Cassiar AK 10.0 Clinton CT 45.0 Cassiar AX 5.0 Cassiar AZ 30.0 Plant 256, Blend 20-3/76 Cassiar AS 10.07. Cassiar AK 10.0 Clinton CT 45.0 Cassiar AK 5.0 Clinton CY 30.0 Plant 258, Blend 64-5/76 Cassiar AK 3.87. JM 4T-30 15.3 Clinton CT 45.7 Clinton CY 11.5 JM 5R-28 3.8 Corp. 4D 11.5 BT/AD Blue 8.4 Plant 258, Blend 94-6/76 Cassiar AK 3.77. Clinton CT 11.0 Corp. 4T 22.1 JM 5R-28 7.4 BT/AD Blue 8.1 Corp. 4j 11.0 Corp. 4D 22.1 Russian P-5 14.6 CTD000902 Plant 257, Blend 61-7/76 Clinton CP 25.77, Cassiar AX 12.9 Clinton CT 25.7 Russian P-5 17.2 Cassiar AZ A.3 BT/AD Blue 14.2 Plant 258, Blend 144-8/76# Cassiar AK 3.77.* Clinton CT 18.4 JM 4T-30 14.7 JM 5R-28 11.0 BT/AD Blue 8.1 Corp. 4T 7.4 Corp. 4D 14.7 Russian P-5 11.0 Cassiar AX 11.0 Plant 260-Blend 49-9/76 Clinton CY 22.9% Clinton CT 42.0 Cassiar AK 15.3 Cassiar AX 7.6 Pacific 5R 3.8 ML-6 Blue 8.4 Plant 257, Blend 105-9/76 Clinton CT 53.8% Russian P-5 31.4 ML-6 Blue 14.8 Plant 257, Blend 125-11/76 Clinton CT 26.9% Russian P-5 17.9 Cassiar AK 26.9 Cassiar AX 13.5 ML-6 Blue 14.8 CTD000903 APPENDIX V Relative Strength Tests on Plant Fiber Blends Plant Blends - 10/74 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 3% Fiber pounds average 97. Fiber pounds average 157. Fiber pounds average 83 81.5 80 113 98.0 83 91 85.0 79 160 154.0 148 156 153.5 151 148 156.5 165 208 207.5 207 245 224.0 203 197 211.5 226 83 154' 88 155 208 214 Plant 256, Blend 17 - Flexural Strength Sample pounds 157. Fiber average 1 227 219.5 212 2 228 233.5 239 3 223 214.5 206 4 214 212.0 210 5 223 219.0 215 6 234 219.5 205 Median Average 219 220 CTD000904 Plant 257, Blend 86 - Flexural Strength Sample 15% Fiber pounds average 1 226 219.5 213 2 235 218.5 202 3 247 232.5 218 4 220 227.0 234 5 228 224.5 221 6 245 227.0 209 Median Average 224 225 Plant 258, Blend 85 - Flexural Strength Sample 15% Fiber pounds average 1 205 215.0 225 2 207 216.0 225 3 223 211.5 200 4 217 224.5 232 5 206 209.0 212 6 247 215.0 183 Median Average 215 215 CTD000905 From Average Standard AX Curve (Using Average Values) Breaking Load 15% Std. AX Breaking Load 0% Fiber Relative Strength Blend17 Relative Strength Blend86 Relative Strength Blend85 215pounds 57 97 100 94 CTD000906 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 37. Fiber pounds average 97. Fiber pounds average 157. Fiber pounds average 70 77.0 84 93 94.0 95 71 79.0 87 164 154.0 214 227.5 144 241 151 150.5 232 227.0 150 222 139 143.5 214 227.5 148 241 86 149 227 83 149 227 Plant 260, Blend 86 (Test #1) - Flexural Strength Sample 157. Fiber pounds average 1 228 211.5 195 2 218 221.5 225 3 245 228.5 212 4 245 232.5 220 5 224 223.0 222 6 239 229.5 220 Median Average 223 224 From Average Standard AX Curve (Using Average Values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength Blend 86 226 pounds 45 93 CTD000907 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 37. Fiber pounds average 97. Fiber pounds average 157. Fiber pounds average 99 101.5 104 104 94.0 84 67 83.5 100 145 149.0 153 156 148.5 141 148 152.0 156 215 213.5 212 218 223.5 229 210 209.0 208 100 151 214 93 150 215 Plant 259, Blend 76 - Flexural Strength Sample pounds 15% Fiber__________ average 1 184 200.0 216 2 210 216.0 222 3 208 209.0 210 4 211 217.5 224 5 231 228.0 225 6 209 215.5 222 Median Average 214 214 From Average Standard AX Curve (Using Average Values) Breaking Load 157, Std. AX Breaking Load 07. Fiber Relative Strength Blend 76 214 pounds 61 94 CTD000908 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 37. Fiber_____ pounds average 97. Fiber pounds average 157. Fiber pounds average 79 78.5 78 71 76.5 82 85 91.0 97 155 164.0 173 154 147.0 140 141 144.5 148 232 220.0 208 246 237.0 228 226 224.5 223 81 151 82 152 227 227 Plant 260, Blend 86 (Test #2) - Flexural Strength Sample 157. Fiber pounds average 1 254 230.5 207 2 254 241.0 228 3 230 232.5 235 4 225 237.0 249 5 240 220.5 201 6 232 228.0 224 Median Average 231 232 - From Average Standard AX Curve (Using Average Values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength Blend 86 227 pounds 45 97 CTD000909 Plant Blend - 8/75 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 37. Fiber pounds average 97. Fiber pounds average 157. Fiber pounds average 84 81.0 78 71 68.5 66 110 105.0 100 164 154.5 145 154 156.5 159 145 155.0 165 223 217.0 211 213 . 213.5 214 224 219.5 215 81 157 215 85 155 217 Plant 257, Blend 115 - Flexural Strength Sample 15% Fiber pounds average 1 241 220.0 199 2 239 215.5 192 3 232 228.5 225 Median Average 229 221 From Average Standard AX Curve (Using Median Values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength Blend 115 217 pounds 49 101 CTD000910 Plant Blends - 12/75 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 37. Fiber pounds average 97. Fiber pounds average 157. Fiber pounds average 66 66.5 67 65 69.5 74 59 58.5 58 127 129.5 132 135 134.5 134 138 142.5 147 214 217.0 220 217 207.5 198 207 201.5 196 66 135 211 65 136 209 Plant 256, Blend 71 - Flexural Strength Sample 15% Fiber pounds average 1 218 217.5 217 2 228 221.5 215 3 223 227.0 231 Median Average 221 222 Plant 257, Blend 187 - Flexural Strength Sample 157. Fiber pounds average 1 246 262.0 278 2 236 244.5 253 3 248 246.0 244 Median Average 247 251 CTD000911 Plant 258, Blend 170 - Flexural Strength Sample 15% Fiber pounds average 1 227 217.5 208 2 241 243.5 246 3 225 218.0 211 Median Average 226 226 Plant 259, Blend 62 - Flexural Strength Sample 15% Fiber pounds average 1 2 3 Median Median Average 236 203 224 257 235 226 231 230 219.5 240.5 230.5 Plant 260, Blend 84 - Flexural Strength Sample 15% Fiber pounds averagi 1 247 232.0 217 2 263 240.5 218 3 265 229.0 193 Median Average 233 234 CTD000912 From Average Standard AX Curve (Using Median Values) Breaking Load 15% Std. AX Breaking Load 0% Fiber Relative Strength Blend 71 Relative Strength Blend 187 Relative Strength Blend 170 Relative Strength Blend 62 Relative Strength Blend 84 210 pounds 28 100 113 102 105 106 CTD000913 Plant Blends - 2/76, 3/76 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 5% Fiber pounds average 10% Fiber pounds average 15% Fiber pounds average 105 97.5 90 94 97.0 100 91 91.5 92 149 142.0 135 172 161.0 150 162 159.0 156 206 205 221 214 207 1900 205.5 217.5 198.5 93 153 207 95 154 207 Plant 257, Standard Blend - Flexural Strength Sample 15% Fiber pound s average 1 255 247.0 239 2 249 243.5 238 3 276 270.5 265 Median Average 252 254 Plant 258, Standard Blend - Flexural Strength Sample 15% Fiber pounds average 1 229 232.0 235 2 255 239.5 224 3 234 233.5 233 Median Average 234 235 CTD000914 Plant 259, Standard Blend - Flexural' Strength Sample 157. Fiber pound s average 1 240 226.5 213 2 263 229.0 195 3 245 238.5 232 Median Average 236 231 Plant 260, Standard Blend - Flexural Strength Sample 157. Fiber pounds average 1 224 226.5 229 2 262 247.5 233 3 240 254.0 268 Median Average 237 243 From Average Standard AX Curve (Using Median Values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength Plant 257 Relative Strength Plant 258 Relative Strength Plant 259 Relative Strength Plant 260 208 pounds 38 118 108 110 110 CTD000915 Sample 1 2 3 Median Average Plant Blends - 3/76, 5/76 Standard Cassiar AX - Flexural Strength 57. Fiber 107. Fiber pounds average pound s average 157. Fiber pounds average 117 114.5 154 157.0 112 160 115 114.5 171 166.5 114 162 115 113.0 165 169.5 111 174 199 211.5 224 253 234.0 215 222 217.0 212 115 164 114 164 219 221 Plant 256, Blend 20X - Flexural Strength Sample 157. Fiber pounds average 1 228 238.5 249 2 245 231.5 218 3 257 224.0 191 Median Average 237 231 Plant 256, Blend 20 - Flexural Strength Sample 15% Fiber pounds average 1 200 211.0 222 2 212 227.5 243 3 229 230.5 232 Median Average 226 223 CTD000916 Plant 258, Blend 64 (11,000 surface) - Flexural Strength Sample pounds 15% Fiber average 1 247 246.5 246 2 237 235.5 234 3 240 252.0 264 Median Average 243 245 Plant 258, Blend 64 (9,300 surface) - Flexural Strength Sample 15% Fiber pounds average 1 200 211.0 222 2 212 227.5 243 3 229 230.5 232 Median Average 226 223 From Average Standard AX Curve (Using Median Values) Breaking Load 15% Std. AX Breaking Load 0% Fiber Relative Strength Blend 2 OX Relative Strength Blend 20 Relative Strength Blend 64 (9,300 surface) Relative Strength Blend 64 (11,000 surface) 218 pounds 63 106 110 99 109 CTD000917 Plant Blend - 6/76 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 57. Fiber pounds average 107. Fiber pounds average 157. Fiber pounds average 113 114.0 115 97 102.0 107 108 99.5 91 177 177.5 178 170 162.0 154 169 164.0 159 250 229.0 208 245 232.0 219 213 218.0 223 108 170 221 105 168 226 Plant 258, Blend 94 - Flexural Strength Sample 157. Fiber pounds average 1 226 229.5 233 2 217 227.0 237 3 237 221.5 206. Median Average 230 226 Fran Average Standard AX Curve (Using Median Values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength Blend 94 223 pounds 54 98 CTD000918 Plant Blend - 7/76 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 5% Fiber pounds average 107. Fiber pounds average 157. Fiber pounds average 99 108.5 118 107 105.0 103 105 110.0 115 174 170.0 166 173 175.5 178 167 166.5 166 219 218.5 218 263 239.5 216 216 209.5 203 106 170 217 108 171 223 Plant 257, Blend 61 - Flexural Strength Sample pounds 157. Fiber average 1 242 263.5 285 2 259 266.0 273 3 286 266.0 246 Median Average 266 265 From Average Standard AX Curve (Using Median Values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength Blend 61 220 pounds 53 120 CTD000919 Plant Blend - 8/76 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 57. Fiber pounds average 107. Fiber pounds average 157. Fiber pounds average 97 105.0 113 110 110.0 110 96 106.0 116 164 171.5 179 158 155.5 153 154 152.0 150 209 217.0 225 200 202.0 204 243 226.0 209 110 156 107 160 209 215 Plant 258, Blend 144 - Flexural Strength Sample 157. Fiber pounds average 1 209 223.5 238 2 198 221.5 245 3 270 231.5 193 Median Average 224 226 From Average Standard AX Curve (Using Median Values) Breaking Load 157. Std. AX Breaking Load 07. Fiber Relative Strength Blend 144 208 pounds 60 104 CTD000920 Sample 1 2 3 Median Average Plant Blends - 9/76 Standard Cassiar AX - Flexural Strength 5% Fiber pounds average 10% Fiber pounds average 15% Fiber pounds average 123 118.0 113 113 112.5 112 107 102.5 98 156 157.5 159 169 161.0 153 173 169.0 165 229 220.0 211 211 215.0 219 228 227.5 227 113 162 223 111 163 221 Plant 260, Blend 49 - Flexural Strength Sample 15% Fiber pounds average 1 235 262.0 289 2 268 267.5 267 3 264 255.5 247 Median Average 266 262 Plant 257, Blend 105 - Flexural Strength Sample 15% Fiber pounds average 1 266 254.5 243 2 258 256.0 254 3 214 245.0 276 Median Average 256 252 CTD000921 From Average Standard AX Curve (Using Median Values) Breaking Load 15% Std. AX Breaking Load 0% Fiber Relative Strength Blend 49 Relative Strength Blend 105 221 pounds 56 120 114 CTD000922 Plant Blend - 11/76 Sample 1 2 3 Median Average Standard Cassiar AX - Flexural Strength 57. Fiber pounds average 100 102.5 105 101 98.0 95 86 93.0 100 100 98 107. Fiber pounds average 150 156.5 163 145 149.0 153 168 160.0 152 153 155 157. Fiber pounds average 194 211.5 229 224 208.5 193 205 210.0 215 210 210 Plant 257, Blend 125 - Flexural Strength Sample __________ 157. Fiber pounds 1 237 248.5 260 2 271 244.0 217 3 241 222.0 203 Median Average 239 238 From Average Standard AX Curve (Using Median Values) Breaking Load 15% Std. AX Breaking Load 0% Fiber Relative Strength Blend 125 209 pounds 45 111 CTD000923