Document 0619pYQwNo4a8mQaqdaogXnEJ

si a) *1\ 1 : Pamela Moseley/DC/USEPA/US 08/28/2008 10:46 AM To Toni Krasmc/DC/USEPA/US@EPA cc Deena Vann/DC/USEPA/US@EPA bcc Subject Fw: LOI Submission of August 1,2008 O Toni, 1. You need to download and print the attached pages 2. Verify that they do not contain CBI 3. Submit them to the CBI Center to get date stamped and a mail receipt number N O TE. The CBIC staff will then send these to me to be coded and the pages will then be replaced THANKS! Pam Moseley TSCA CBI Access Coordinator OPPT/IMD/RDMB [7407Mj EPA East Room 6104 1200 Pennsylvania Ave, NW Washington, DC 20460-0001 202-564-8956 202-564-8955 (FAX #] -- Forwarded by Pamela Moseley/DC/USEPA/US on 08/28/2008 10:43 AM -- * i a I Deena Vann /DC/USEPA/US 08/28/2008 10:18 AM To Tom Krasmc/DC/USEPA/US@EPA cc Pamela Moseley/DC/USEPA/US@EPA Subject Re: Fw: LQl Submission of August 1, 200&Q Hi Toni, The document hasn't been transferred to NCIC yet, so it is still here in our office. You should talk to Pam Moseley in RDMB about making changes to the document. Deena W. Vann TSCA CBIC Program Manager (202) 564-8932 Contractor to EPA ASRC Aerospace Corporation Toni Krasnic/DC/USEPA/US Toni Krasnic/DC/USEPA/US 1 ISO ON SNIV1NOO 08/27/2008 01319 PM J -jTo Deena Vann/DC/USEPA/US@EPA *-cc Subject Fw; LOI Submission of August 1. 2008 Hi Deena, 3M sent this to EPA around August 1,2008. If the submission has not yet been processed into the docket, is it possible to replace the last two pages with the corrected pages attached below? If it's too late, I can have them submit the correction through the regular submission process. Thank for your help, Toni Krasnic EPA/OPPTS/OPPT/CCD/ECB EPA East; 1201 Constitution Ave NW, Room 4410L; Washington, DC 20004 Mail: EPA; 1200 Pennsylvania Ave NW; MC-7405M; Washington, DC 20460 Phone: 202-564-0984; Fax: 202-564-477S PFOA Website: http://www.epa.oov/QPDt/Dfoa TSCA 8(e) Website: h tto ;//www.eoa.oov/opotintr/tscaBe -- Forwarded by Toni Krasmc/DC/USEPA/US on 08/27/2008 01:09 PM -- m8santoro@mmm.com 08/27/2008 12:13 PM To Toni Krasnic/DC/USEPA/US@EPA cc Subject LOI Submission of August 1. 2008 Toni, regarding our telephone conversation attached is a copy of the original LOI submission of August 1, 2008, along with the corrected 2 pages of Table 6. These are the last two pages of the report. Thank you for ycur assistance in assuring that the corrected version is entered into the Docket. Sincerely Mike Michael A. Santoro Director, Environmental, Health, Safety and Regulatory Affairs 3M Enterprise Services Bldg. 236-1B-10 Tel: 651-733-6374 Fax: 651-733-1958 Notice: This e-mail, including any attached files, contains information that may be confidential. It is intended to be a private communication only for the recipient(s) named above. If you are not an intended 3V Ge'o'al Otfi.'es 3M Ce'.te St Pajl. MN 55l-*-*-lOOO 551 733 1110 August !. 2008 VIA UPS Document Control Office (DCO) Office ol Pollution Prevention and Toxics (OPPT) US Environmental Protection Agency EPA East. Room 6428 1201 Constitution Avenue, NW Washington DC 20460 Attention: Docket No. AR-226 and the PFOA Electronic Docket OPPT-2003-0012 Subject: Submission of Monitoring Daia Pursuant to the 3M LOI dated March 13, 2003 and PFOA Users LOI dated March 14. 2003 Dear Sir or Madam: This report is submitted pursuant to the 3M Letter of Intent (LOI) dated March 13. 2003 and the PFOA Users LOI dated March 14, 2003. On August 1, 2007, 3M/Dyneon submitted the final report of the results of groundwater and wastewater monitoring at the 3M manufacturing sites at Cottage Grove, NfN and Decatur, AL. However, as stated in that submittal and as indicated in the supplemental letter of May 07, 2003, 3M was to have conducted an additional round of sampling for fish, clams, and Tennessee River water and sediment in the vicinity of the Decatur. Alabama manufacturing facility. This sampling occurred in December of 2006. In this submittal we are providing the results of the analyses of perfluorooctanoic acid (PFOA) for these samples. The water and sediment data is shown in Table 5 attached, which includes the data from sampling conducted previously. The fish and clam data from sampling in December, 2004 (submined previously) and from the more recent sampling in December 2006 is shown in Tabic 6. In summary, this submittal fulfills all commitments of 3M and Dvneon under the March 13, 2003 3M LOI and the March 14, 2003 APFO Users LOI. If there are any questions, please contact the writer at the address provided below. Sincere!). - Michael AjSantoro Director, Environmental, Health, Safety and Regulatory Affairs 3M - Bldg. 236-IB-10 St. Paul, MN 55144 651 733-6374 (phone) 651 733-1958 (fax) E-mail: m^rinur <.... ' cc: Toni Kxasnic - Room 4410 (w / attachm ents) S a m p le L o c a tio n L O C -3 . R rv er M ie 9 0 7 5 L O C -2 . R iv e r M e 3C 1 IO C -1 . R iv e r M e 2 fi6 T a M e S . M l D e c a tu r- S u rfa c e W a te r A S e d im e n t M o n ito rin g R eeuM D a ta S a m p le d M edi 2002 1 2 * 0 1 :0 4 1 2 /1 /2 0 0 6 2002 1 2 /0 1 /IM 1 2 * 0 1 /0 6 2002 1Tn S u rfa ce w a te r S u rfa c e w a te r S eg m en t Loe 1 S edm ent L oc2 S e d im e n t L oc 3 S u rfa c e w a te r S e d im e n t L o c S e d im e n t L oc 2 Sodm am . Loc 3 S u rfa c e w a te r S u rfa c e w a te r S odm ant Loc 1 S o d m o n t. lo c 2 S edm ent L oc3 S u rfa c e w a te r S o d m a n t to c 1 S e d im e n t. L o c 2 S e d im e n t lo c 3 1 S u rtac e w a to r | S u rfa c e w a te r { S e d im e n t L o c i j S e d im e n t L oc 2 j S edenent Loc 3 1 S u rfa ce w afer ' Sedenent Loc 1 < S e d a n e n t. L o c 2 ! S ed an # - loc 3 P F O A (ppb) PFO A U b R e p lic a le lo o t P F O A H e ld D u p lic a te ( p p b ) P F O A A v g |p p t> ) NO ND ND NO ND NO ND NC ND ND ND NC NO ND NO NC ND ND NO ND NO NO ND NC NO ND ND NC NO ND NO NC ND I ND NO ND ND ND NO 1 11 N O NO NO NO ND ND NO ND NO i ND NC ND NC NO NC NO NC <0 66 NC NO NC ND NC ND NC NO I 020 0 16 0 19 0 2 0 0 1 NO NO NC NQ 1 54 1 93 0 9631 0 566 1 0 .9 3 S NC 124 1 90 NC 1 67 0 0 6 6 7 N C 0 .0 7 6 4 0465 NC 0536 0 463 ! n: ' 0 .7 S 2 NO NO NC ND ppe. p H piT C S on [ ubA. fix w ater, n ^ g (w et wgQ fix aedm ent) N C -noi cotecM d NO 00 detecte d a t or m ove 0 025 u p l lo r w ater. 041 ng 'g to r sedim ent NO: not quanM ebte. r**U t is betw een 0.2 and 0.4 n p o [w et w gt) CONTAINS NO CB Table 6. 3M Oecatur Fiab and Clama M en toring Reeulta Sample Locaban Speda Sample Type I Sample O Channel Cateti LargemoiXft Bau Channel Catfish Largemoutfi Bau i j 1 Cnenner Catien Largement! Barn . AaeteClam Flat Whole Boay Fret W hdeBody Whom Boev Fret Whom Body Ftet Whole Body Fiet Whole Body Fret Whole Body Whom Body OLS-F01-IFF002-0-W102t CL1-F01-'P*OC5-2-041021 OL5-F01-/PF004-0-041Q21 C -.S .*0 1lP F 'S -0 -0 4ia? l C . J-BV - "//DO1-C-0T1* 50 OL>FC1-lPW002-0-0*1130 DLl-FO NIPW003-0-04 11JO OLS-F01-/PVW04-O-O41 1JO DLJ-F01-tPW005-0-0*25l DL3-F01-U.F001-M/411C5 CMJ-F01-MSF002-0-041105 OL3-F01-MSFOOWWM1105 Ol 2*01-USF004-0-04 1 tos DL3-F01-MSF005-0-0411G5 OL3-F01-MSWOC1-0-04110 OlVf01 -M SW 00 2> 0-0 41 lO S DL3-F01-4ISW0OJ-O-O41105 OL3-F01-MSW004-0-04110S 01 5-M JdSWOOVO-n 1 10? O L >to i-crw o i-a e i2 io C _2c Ct-*PF%1 3 0 1 'n ;" OL2-F01-/PFOQ2-O-<Mi CC1 DL2 -F01-'P * 303-0-041021 DL7-F01-1PFC04-04W1021 D.2-F01-IP*005-(W41?1 Ol 2-F01JPW0C1-O*4102: D L 2 -f 0 1 -/P W X 2 -0 -0 * 1 1 '3 * Dt_2-F01-tP\Y:C5-0-0t21 0L2-F0 iJPW OOd^O* 1215 Dt2-F01-IPWeC5N0171S c : J-F 01-MSF0&4-0- M 10i l DL2-F01-USF002-0-C41021 DL2-F01-MSF003-0-CM1021 OL2-F01-MSF004^N01021 D.2-F01-MSF006-0-C41216 CL? ? v i WSW001-0041C21 OL2-F01-MSW0C2-O-OI1C2: DL2-F01-MSW003-0-0 1C21 D12-f o v m Swoo*- o-04i i D L 2 ^0 1-M S W M W -0 41 :- 21 OL2- to i- c rw o o t- o e i2 i t D.1FJ1.IPF001 5-CMiOil OL1-FO1-1PF032-4NO411C4 DL1-F01-IPFOOJ-lWM1 1Cm DL1-F01-IPF004-0*4 11CM D LTS -iP P oFo-oruoe DL t-F 3 .|PW ;o 1-0-0* 11M DL1-F01-/PW002-0-041 '0 OL1-F01-IPW005-OMM11<M Dl1-FOl-PW004-0-04110e DL1-FOl-tPWOOS4!W>1?1S OL1-FC1-MSFC01-0-041154 DL1-F01-MSF0C2-O-O41154 DL1.F01-MSF003-0-04115 D v l-F 0 1 .I F O O *^ M M 1 1 J 4 OL 1-F01-MSF0OS-O^4114 OL1-F91-MSW0O144411O4 OL 1-F31-MSW0020^4110 OL1-FC1-M$W0O-O-O110 OL1-FC1-MSW004-0-04110 OL 1-F01-I4SWQ0S4LO411O DL1-)01-CFW001-04121S Date Sampled | 0 7 '..'04 1071 4 10/21 04 1071/0 1071.0 1170104 1 1 'JO*/ 1170.0 11.70.04 12 0 1/0 1105/04 110504 110504 1*060 11050 110504 11.050 M .0504 110504 11.0504 12 *0717 107104 107104 107tO4 '0 7 1 0 4 1 0 .-1 0 11.040 12 0 10 12*1504 12-130 10 210 10710* 10710 12H04 1071.0 107104 107104 107104 10.71/04 12 16 0 ' 0210 11 ,0 4 0 * 11.040 11,040 11.040 -1 n*o 11040 11.040 11/0404 12150 11 540 11040 11.040 11.040 11.0404 11/0404 11,040 11.040 11/040 11.0404 12160 PFQA (ppb) UJ 0 556 NO NO NO .T no NO NO NO NO NO NO NO NO NO NO NO NO NO *c, ` .C NO NO NO NC ,n NO NC NO NC NC NC NC NO NC \L NO NO NC NC <536 1.6 NO NC NO NC s-C 0.764 NO NO NC NT NO NO NO NO UZ NO NC NO NO NC 1 PF04 U b 1 Raobcata (sebi N ND NO NO NO -.3 NO NO NO NC NO NO NC NC NC NO NO ND ND NO ; j *.C ND NC NC ND NO ND ND ND NO NO NO ND ND NO V) ND NO NC ND \j KZ NO NO ND ND NO 0 764 NC NO NO m:. HO NO ND ND n: ND NO NQ NO O.SCS Table Nom: ape- pf per Mtacn (ug/l) MO.fwca--cnaaqritwi c.2ng MO netquarntieMe. meaeumd eawctwr i w o e f --n o 2 and 0 6 VB 7L^ C t Table 6 Continued Fish Fillet and Whole Body PFOA Concentrations December 1, 2006 L O C -3 . R iv e r M ile 3 0 7 5 L O C -2 , R iv e r M ile 3 01 S em p le II) S p e c ie s D i3 -F o :-;rro o i-o -0 6 !2 ii D L 3-R )2*IP F 002-0-0612 I2 D IJ-F 02-iP I)03-0-Q 6lZ I2 D I.3 -F O 2 -'l'r. r 4 -0 -O 6 l2 l2 n i j - i - 0 2 .: n ' 5 -0 -0 6 I2 I2 D I.3 -F 0 2 -IP W 0 0 I-0 -O 6 1 2 I2 D L 3 I '.>2-1P W 0 0 2 - 0 - 0 6 1 2 12 D L 5-F 02-IPW 003-0-061212 1>I .3 - K 0 2 - IP W 0 0 4 - 0 - 0 6 1 2 1 2 D L 3 -F Q 2 -IP W 0 0 5 -0 -0 6 1 2 12 O lJ -ro :..M T 'i 'l l . 0-061207 1)1.3-1 0 2 - M 5 F 0 0 2 - 0 - 0 6 1207 D L 3-I 02 -M > ! <>03-0-061207 IM .3 -F 0 2 -M S K 0 0 4 -0 -0 6 J2 0 7 1)1.3-F02-M S rX > 5-0-061207 D L 3-I02-M SW O O I-0-06I207 I-3 -1-02-M S W 002-0- 6I207 DL 3 -F02 -M S W 003-0-061207 D l.3 -r0 2 -M S \\'0 0 4 -0 .0 0 !2 0 ? 1)1.3 -1* 0 2 -V IS W 0 0 5 - 0 - 0 6 1 2 0 7 D I.3-102- F WOUI -0-061219 IJI.2-F 02-IIM n |.i* .irf.!:i 9 l)l.2 -l:0 2 ;P F 0 0 2 -0 -0 6 I2 0 9 D L2-H J2-1PFW 3-0-06I2 9 D I. 2-102-1P F 0 0 4 -0 -0 6 1209 D I.2 -F 0 2 -IP H X )5 -0 -0 6 l 209 D L 2 -F 0 2 -IP W 0C 1-0 - 0 6 12 0 9 ;>i . 2 - i o 2 . i p \ v o r ; 2 - o -0 6 1 :o<> D L 2-F02-IP W 003-0-061209 D !.2 -l'(i2 -IP W 0 0 4 -0 -n 6 i:0 9 D L 2 F 0 2 -IP W 0 0 5 -0-061200 A siatic C lem C h en n el catfish S em p le T ype rille t W h o le bo d y F illet W h o le bod y W hole B ody F illet W h o le bo d y F illet PFO A (ppb) ND ND ND ND ND 0 .2 6 2 0.371 0.2 X 5 0 .2 5 2 0 .5 5 7 \D ND N I) 201 ND 0 .2 9 1 0 333 0 342 0 351 0 .4 9 7 0 .2 2 ND ND ND ND N I) ND ND ND ND ND PFOA U b R ep licate iD Pb) ND ND ND ND ND 0 .2 5 0 0 .2 0 1 0334 0575 0 492 ND ND ND ND ND 0 367 0 465 0 463 0310 0 462 0218 ND ND ND ND ND ND ND ND NO ND D L2-I02-M SW O O I-0-06I211 D I.2-F 0 2 -M S W 0 0 2 - -0 6 I2 1 1 W h o le bod y 0 .5 2 2 0.591 0 .2 3 1 0 .5 0 9 D L M 02-C F W O O I-0-06I219 A sietlc C lam W h o le body 0 .4 2 4 0 295 I fr d P-5 Table 6 Continued - Fish Fillet and Whole Body PFOA Concentrations December 1, 2006 L O C -3 , R iver M ile 3 0 7 .5 L O C -2 , R iv er M ile 301 ,-V -. S am p le ID S p e c ie s Sam ple T ype D L 3-F02-IPF00I-0-06I2II D l .3 - F 0 2 - 1P F 0 0 2 - 0 - 0 6 1212 D L3-F02-IPF003-0-06I2I2 D L3-F02-IPF004-0-061212 D L3-F02-1PF005-0-061212 D 1 .3 -F 0 2 -IP W 0 0 1-0 -0 6 1 2 1 2 D L3-F02-IPW 002-0-0612I2 D L 3-F02-IP W 003-0-061212 D L 3-F02-IP W 004-0-061212 D L 3-F02-IP W 005-0-061212 D L 3 - F 0 2 - M S F 0 0 1-0 -0 6 1 2 0 7 D I.3-F02-M S F002-0-06I207 D L 3-F02-M SF003-0-061207 Dl .3-F 02-M S F004-0-061207 D L 3-F 02-M S l:0 0 5-0-061207 D L 3 -1 -0 2 -M S W 001 - 0 - 0 6 12 0 7 D I.3-F02-M SW 002-0-061207 D I.3-F02-M SW 003-0-061207 DL3-1-02-M S W 004-0-061207 D L 3-F 02-M S W 005-0-061207 C hannel catfish L argem outh bass D 1 .3 -102-C FW O O I -0 -0 6 1 2 1 9 DL2-F02-1PF001 -0-061209 D L2-F02-1PF002-0-061209 D L 2-F 0 2 -1 P F 0 0 3 -0 -0 6 1 2 0 9 D L 2-F02-IP F004-0-061209 D L 2-F02-IP F005-0-061209 D1.2-F02-IP W 001-0-061209 D 1.2-F02-IP W 002-0-061209 D 1.2-F02-IPW 003-0-06I209 D L 2-F02-IP W 004-0-061209 Dl .2-F02-IP W 005-0-061209 N ot Sam pled N ot Sam pled N ot Sam pled N ot Sam pled N ot Sam pled D L 2-F 02-M S W 001-0-061211 D 1.2-F02-M SW 002-0-061211 N ot Sam pled N ot Sam pled N ot Sam pled A siatic C lam C hannel catfish L argem outh bass D L2-I02-C FW 001 -0-061219 A siatic C lam Fillet W hole body F ille t W hole body W hole Body F ille t W hole body Fillet W hole body W hole body PFOA (ppb) ND ND ND ND ND ND ND ND ND ND 0.434 ND 0.359 0.319 ND ND ND ND ND ND PFOA Lab R eplicate (ppb) ND ND ND ND ND ND ND ND ND ND 0 .5 0 3 ND 0 .3 8 1 0 .2 7 0 ND ND 0 .3 8 6 ND ND ND 0.22 ND ND ND ND ND ND ND ND ND ND - - - - 0.522 0.591 - - - 0 .2 1 8 ND ND ND ND ND ND ND ND ND ND * - - 0.231 0 .5 0 9 0.424 0 .2 9 5 o .o ~6 i o CONTAINS NO OB' CJ ro P-6 L O C -1 , R iver M ile 2 9 6 D L I-F O 2-IP F 0O I-O -O 6I2I2 D U -F 02-IP F 002-0-061212 D I.I-F O 2 -IP F O 0 3 -O -O 6 1 2 1 2 F ille t DI .I-F 02-IPF 004-0-061212 D L1-F02-IPF005-0-061212 D L1-F02-1PW 001-0-061212 D L 1- F 0 2 -1 P W 0 0 2 -0 -0 6 1212 D1.1-F02-1P W 003-0-061212 1)1,1-F02-IP W 004-0-061215 D L 1-F 0 2 -IP W 0 0 5 -0 -0 6 1215 D I.I-F02-M SF001-0-061209 D I.I-F02-M SF002-0-061209 D LI-F02-M SF003-0-061209 D L1-F02-M SF004-0-06I209 D -F02-M SF005-0-061209 DL1-F02-M SW 001-0-061209 D L 1-F 0 2 -M S W 0 0 2 -0 -0 6 1209 D L 1-F 0 2 -M S W 0 0 3 -0 -0 6 1 20 9 D L 1-F 0 2 -M S W 0 0 4 - 0 -0 6 1209 D L 1-F 0 2 - M S W 0 0 5 - 0 - 0 6 1209 C hannel catfish L argem outh bass W hole body F ille t W hole body D LI-102-C FW 001-0-061219 A siatic C lam W hole body Fish issue concentrulions reported on a wel weight basis. ND = Not detected at or above 0.2 ng/g. NR = Not reported due to quality control failures. ND ND ND ND ND 0.262 0 .3 7 1 0.285 0.252 0.557 ND ND ND 0 .2 0 1 ND 0.291 0.333 0.342 0.351 0.497 ND . ND ND ND ND ND 0 .3 5 0 0 .3 0 1 0 .3 3 4 0 .2 7 5 0 .4 9 2 ND ND ND ND ND 0 .3 8 7 0 .4 8 5 0 .4 6 8 0 .3 1 0 0 .4 8 2 0 .2 2 1